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Finally shut off the cooling water circulation. This is important, because if you are using plastic tubing to collect the distillate from the condenser, it could get kinked or obstructed in some way. That would seal off the apparatus from the air. If this happened while it was cooling down, a vacuum would be formed within the still as the vapors inside condense, and the air pressure outside could crush the unit. When the unit has reached room temperature, disconnect the cooling hoses, backflush the column with water then remove the top end from the boiler for cleaning.

The remainder is re-cycled back into the column. This controls the amount of refluxing. The proportion of distillate returned to the column versus that which is withdrawn is called the Reflux Ratio. In theory, the more reflux cycles that are allowed to take place the purer the output will be. In other words, high reflux ratios produce more refined products. In practice though, you will find that as you increase the reflux ratio more and more, it produces less and less improvement in the purity of the output.

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