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Download Methods of Biochemical Analysis, Volume 10 by David Glick PDF

By David Glick


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Components A, C, and E were collected from the gas stream and identified as crystalline derivatives. The quantities of components B and D were too small to permit unequivocal identifications, but component D was identical on gas-liquid partition chromatograms with an authentic sample of methyl 2,3,6-tri-O-methyl-a-~-mannopyranoside. The relative degree of simplicity of this chromatogram in comparison with those from other methylated polysaccharides (Fig$. 9-12 and 14) is a result of the formation of only one anomer from the mannose derivatives.

31, 486 (1961). 28. , and G. A. Adams, Can. J. , 39,889 (1961). 29. , H. Trischmann, and I. Low, Angew. , 67,32 (1955). 30. Lovelock, J. , J. , i, 35 (19%). 31. McInnes, A. , D. H. Ball, F. P. Cooper, and C. T. Bishop, J . , 1, 556 (1958). 32. McWilliam, I. , and R. A. Dewar, in D. H. , Gas Chromatography, Vol. 2, Butterworths, London, 1958, p. 142. 33. Ormerod, E. , and R. P. W. Scott, J. , d,65 (1959). 34. , and C. T. Bishop, Can. J. , 39,815 (1961). 35. sChromatography, Butterworths, London, 1956.

B. MERCURATED ALLYLAMIDES These compounds, which are made by the mercuration of an olefinic double bond, have been employed clinically as diuretics for a long time (95).

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